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Please use this identifier to cite or link to this item: http://repository.li.mahidol.ac.th/dspace/handle/123456789/31510
Title: Synthesis of gem-difluoromethylenated spiro-γ-butyrolactones by employing PhSCF<inf>2</inf>Si(CH<inf>3</inf>)<inf>3</inf>as a gem-difluoromethylenating agent
Authors: Adisak Chatupheeraphat
Darunee Soorukram
Chutima Kuhakarn
Patoomratana Tuchinda
Vichai Reutrakul
Chaveng Pakawatchai
Saowanit Saithong
Manat Pohmakotr
Mahidol University
Prince of Songkla University
Keywords: Chemistry
Issue Date: 1-Oct-2013
Citation: European Journal of Organic Chemistry. No.30 (2013), 6844-6858
Abstract: PhSCF2TMS was utilized as a useful gem-difluoromethylene building block for the synthesis of gem-difluoromethylenated spiro-γ-butyrolactones. The radical cyclization of γ-alkenyl- γ-gem-difluoro(phenylsulfanyl)methyl-γ-butyrolactones provided gem-difluoromethylenated spiro-γ-butyrolactones. PhSCF2TMS (TMS = trimethylsilyl) is utilized as a gem-difluoromethylenating agent for the synthesis of gem-difluoromethylenated spiro-γ-butyrolactones. Copyright © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
URI: https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84885597753&origin=inward
http://repository.li.mahidol.ac.th/dspace/handle/123456789/31510
ISSN: 10990690
1434193X
Appears in Collections:Scopus 2011-2015

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