Publication: Effect of micro-arc oxidation time on the Ca-P coating layer properties formed on commercially pure titanium
Issued Date
2010-10-22
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16800737
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2-s2.0-77958010844
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Mahidol University
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SCOPUS
Bibliographic Citation
IFMBE Proceedings. Vol.31 IFMBE, (2010), 1200-1203
Suggested Citation
P. Katekaew, W. Veerasai, A. Aeimbhu Effect of micro-arc oxidation time on the Ca-P coating layer properties formed on commercially pure titanium. IFMBE Proceedings. Vol.31 IFMBE, (2010), 1200-1203. doi:10.1007/978-3-642-14515-5_304 Retrieved from: https://repository.li.mahidol.ac.th/handle/20.500.14594/28888
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Title
Effect of micro-arc oxidation time on the Ca-P coating layer properties formed on commercially pure titanium
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Abstract
In the present study, the Ca-P coating layer on commercially pure titanium was fabricated using Micro-arc oxidation (MAO) method in electrolyte for osteointegrative coating (ESOC) at constant potential for different periods of time (0 - 600 minutes). The morphological microstructures, crystal structure and roughness of Ca-P coating layers were characterised by Scanning Electron Microscopy (SEM), Energy Dispersive X-ray Spectrometer (EDS), X-ray Diffraction technique (XRD) and Atomic Force Microscope (AFM). SEM micrographs of treated samples demonstrated the microporous structure of Ca-P coating layer. Moreover, the results indicated that the number and size of micropores have increased with an increasing oxidation time. The contents of Ca and P on coating layer depend on the oxidation time. XRD results showed that the fabricated Ca-P coating layer contains Ti and hydroxyapatite (HA) phases at t = 600 minutes. AFM analysis showed that a mean roughness of untreated was 13 nm and treated samples ranging between 80-190 nm. Wettability property of an untreated and treated sample was hydrophilic which the magnitude was no different. © 2010 International Federation for Medical and Biological Engineering.