Publication: Spherical nanocrystalline barium zirconate titanate prepared by Co-precipitation in highly basic aqueous solution
Issued Date
2013-01-01
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ISSN
15635112
00150193
00150193
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2-s2.0-84891762280
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Mahidol University
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SCOPUS
Bibliographic Citation
Ferroelectrics. Vol.455, No.1 (2013), 83-89
Suggested Citation
Panpailin Seeharaj, Supamas Wirunchit, Piyanut Charoonsuk, Pattaraporn Kim-Lohsoontorn, Naratip Vittayakorn Spherical nanocrystalline barium zirconate titanate prepared by Co-precipitation in highly basic aqueous solution. Ferroelectrics. Vol.455, No.1 (2013), 83-89. doi:10.1080/00150193.2013.844054 Retrieved from: https://repository.li.mahidol.ac.th/handle/20.500.14594/32003
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Title
Spherical nanocrystalline barium zirconate titanate prepared by Co-precipitation in highly basic aqueous solution
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Abstract
Spherical monosized barium zirconate titanate nanoparticles (Ba(ZrxTi1-x)O3(BZT) when x = 0.25, 0.30 and 0.35) have been prepared by co-precipitation in a strongly alkaline solution (20 M NaOH) at 80°C. The phase formation of the as-precipitated powders was characterized by XRD, FT-IR and Raman spectroscopy as a single-phase BZT with cubic perovskite oxide structure. This indicates that crystalline BZT powders can be obtained from the co-precipitation in 20 M NaOH without the requirement of calcination process. SEM analysis showed that BZT had nanosized spherical morphology with uniform shape and size. The crystal sizes obtained by TEM analysis were 20-40 nm. © 2013 Copyright Taylor and Francis Group, LLC.