Publication: One-pot synthesis of halogen exchanged silsesquioxanes: Octakis(3-bromopropyl)octasilsesquioxane and octakis(3-iodopropyl) octasilsesquioxane
| dc.contributor.author | V. Ervithayasuporn | en_US |
| dc.contributor.author | N. Pornsamutsin | en_US |
| dc.contributor.author | P. Prangyoo | en_US |
| dc.contributor.author | K. Sammawutthichai | en_US |
| dc.contributor.author | T. Jaroentomeechai | en_US |
| dc.contributor.author | C. Phurat | en_US |
| dc.contributor.author | T. Teerawatananond | en_US |
| dc.contributor.other | Mahidol University | en_US |
| dc.contributor.other | Chulalongkorn University | en_US |
| dc.date.accessioned | 2018-10-19T04:46:54Z | |
| dc.date.available | 2018-10-19T04:46:54Z | |
| dc.date.issued | 2013-10-07 | en_US |
| dc.description.abstract | Metal halides, solvent effects, phase transfer catalysts, alkylating agent and reaction times were found to have important roles to complete halogen exchange reactions in "one pot" synthesis, starting from octakis(3-chloropropyl)octasilsesquioxane to obtain more reactive halide compounds: octakis(3-bromopropyl)octasilsesquioxane and octakis(3-iodopropyl) octasilsesquioxane. To confirm the complete halogen exchange, the desired products were characterized by1H,13C and29Si NMR spectroscopy, ESI-MS, elemental analysis and single-crystal X-ray diffraction analysis. © 2013 The Royal Society of Chemistry. | en_US |
| dc.identifier.citation | Dalton Transactions. Vol.42, No.37 (2013), 13747-13753 | en_US |
| dc.identifier.doi | 10.1039/c3dt51373d | en_US |
| dc.identifier.issn | 14779234 | en_US |
| dc.identifier.issn | 14779226 | en_US |
| dc.identifier.other | 2-s2.0-84883523136 | en_US |
| dc.identifier.uri | https://repository.li.mahidol.ac.th/handle/123456789/31509 | |
| dc.rights | Mahidol University | en_US |
| dc.rights.holder | SCOPUS | en_US |
| dc.source.uri | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84883523136&origin=inward | en_US |
| dc.subject | Chemistry | en_US |
| dc.title | One-pot synthesis of halogen exchanged silsesquioxanes: Octakis(3-bromopropyl)octasilsesquioxane and octakis(3-iodopropyl) octasilsesquioxane | en_US |
| dc.type | Article | en_US |
| dspace.entity.type | Publication | |
| mu.datasource.scopus | https://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=84883523136&origin=inward | en_US |