Publication: Flowsheet synthesis and complex distillation column design for separating ternary heterogeneous azeotropic mixtures
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Issued Date
2011-08-01
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ISSN
02638762
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2-s2.0-79958712595
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Mahidol University
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SCOPUS
Bibliographic Citation
Chemical Engineering Research and Design. Vol.89, No.8 (2011), 1362-1376
Suggested Citation
Paritta Prayoonyong, Megan Jobson Flowsheet synthesis and complex distillation column design for separating ternary heterogeneous azeotropic mixtures. Chemical Engineering Research and Design. Vol.89, No.8 (2011), 1362-1376. doi:10.1016/j.cherd.2011.02.015 Retrieved from: https://repository.li.mahidol.ac.th/handle/123456789/11677
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Title
Flowsheet synthesis and complex distillation column design for separating ternary heterogeneous azeotropic mixtures
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Abstract
The boundary value method for design of distillation columns separating ternary heterogeneous azeotropic mixtures is extended to include complex configurations, i.e. columns with integrated decanters and with multiple heterogeneous stages; double-feed columns; columns with intermediate decanters. The methods can be used for establishing product feasibility in a column and evaluating a column design in terms of cost. Multiple feasible designs can be generated for a given set of product specifications, according to the reflux ratio, number of heterogeneous stages and liquid phase ratio; these designs may be evaluated with respect to operating and equipment costs. Case studies illustrate the design method.An algorithmic approach is presented for synthesising novel sequences for separating, by distillation and decanting, ternary heterogeneous azeotropic mixtures. Existing synthesis procedures that consider only simple single-feed columns with decanters and integrated decanters are extended to include more industrially relevant options such as columns with several heterogeneous stages, double-feed columns, columns with intermediate decanters, and those accepting a heterogeneous liquid feed. With these advanced column configurations included in the synthesis method, a wider range of sequences may be considered systematically, allowing sequences that are more economically attractive than conventional designs to be identified. A case study illustrates the approach. © 2011 The Institution of Chemical Engineers.