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Preparation of [4‐<sup>3</sup>H]‐3‐dehydroretinol by sodium borotritide reduction

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dc.contributor.authorPichit Tosukhowongen_US
dc.contributor.authorThararat Supasirien_US
dc.contributor.otherMahidol Universityen_US
dc.date.accessioned2018-10-12T07:47:36Z
dc.date.available2018-10-12T07:47:36Z
dc.date.issued1985-01-01en_US
dc.description.abstract[4‐3H]‐Dehydroretinol (5) was prepared from a vitamin A derivative. The procedure involves conversion of methyl retinoate (1) to methyl 4‐oxoretinoate (2) by manganes dioxide oxidation. The 3H‐label was introduced by sodium borotritide reduction of methyl 4‐oxoretinoate (2) followed by acid catalyzed dehyration to methyl [4‐3H]‐3‐dehydroretinoate (4). Reduction of the tritiated methyl dehydroretinoate with lithium aluminium hydride yielded [4‐3H]‐3‐dehydroretinol (5). Final purification was achieved by preparative thin layer chromatography. Copyright © 1985 John Wiley & Sons, Ltd.en_US
dc.identifier.citationJournal of Labelled Compounds and Radiopharmaceuticals. Vol.22, No.9 (1985), 925-930en_US
dc.identifier.doi10.1002/jlcr.2580220908en_US
dc.identifier.issn10991344en_US
dc.identifier.issn03624803en_US
dc.identifier.other2-s2.0-0021829501en_US
dc.identifier.urihttps://repository.li.mahidol.ac.th/handle/20.500.14594/30754
dc.rightsMahidol Universityen_US
dc.rights.holderSCOPUSen_US
dc.source.urihttps://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=0021829501&origin=inwarden_US
dc.subjectBiochemistry, Genetics and Molecular Biologyen_US
dc.subjectChemistryen_US
dc.subjectMedicineen_US
dc.subjectPharmacology, Toxicology and Pharmaceuticsen_US
dc.titlePreparation of [4‐<sup>3</sup>H]‐3‐dehydroretinol by sodium borotritide reductionen_US
dc.typeArticleen_US
dspace.entity.typePublication
mu.datasource.scopushttps://www.scopus.com/inward/record.uri?partnerID=HzOxMe3b&scp=0021829501&origin=inwarden_US

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